Chemistry, 03.07.2021 19:50 MeIsBella

What are the methods used to determine the boiling point of a compound?

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There are a variety of methods by which a sample's boiling point can be determined, including distillation, reflux, and by using a Thiele tube. The most straightforward method uses a Thiele tube, and has the advantage of using less than 0.5mL of material.

Distillation Method

There are simpler methods than a distillation to measure a compound's boiling point, and it is recommended to explore other options (e.g. Thiele tube) if this is the only goal. However, if materials are limited, or if a purification is planned anyhow, a distillation can be used to determine a compound's boiling point. The distillation technique is discussed in great detail in Chapter 5.

A simple distillation should suffice for most situations and at least 5mL of sample should be used in the distilling flask along with a few boiling stones or stir bar. As the bulk of the material distills, the highest temperature noted on the thermometer corresponds to the boiling point. A major source of error with this method is recording too low a temperature, before hot vapors fully immerse the thermometer bulb. 5 Be sure to monitor the thermometer periodically, especially when the distillation is active. Record the barometric pressure along with the boiling point.

Reflux Method

A reflux setup can also be used to determine a compound's boiling point. Reflux is when a liquid is actively boiling and condensing, with the condensed liquid returning to the original flask. It is analogous to a distillation setup, with the main difference being the vertical placement of the condenser.

Thiele Tube Method

Answer from: bankskry

There are a variety of methods by which a sample's boiling point can be determined, including distillation, reflux and by using a Thiele tube. The most straightforward method uses a Thilele tube, and has the advantage of using less than 0.5ml of material.

Answer from: Quest

cytokinesis is the splitting of a cell membrane to form 2 identical daughter cells. it's similar to mitosis as both cells have identical copies of dna and cytokinesis is a step in the mitotic cycle.

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i just calculated it all out, and not including weekends, and all the different days off. as of this school year (2018-2019) students are spending 2198 hours in school this year

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